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7.1 The particle size distribution of powdered ion exchange resins and, more importantly, the derived parameters of mean particle size and percent above and below specified size limits are useful for determining batch to batch variations and, in some cases, can be related to certain aspects of product performance.7.2 Although automatic multichannel particle size analyzers, of the type described in Section 9, yield information on the entire distribution of sizes present in a given sample, it has been found that, for this application, the numerical value of three derived parameters may adequately describe the particle size characteristics of the samples: the mean particle diameter (in micrometres), the percent of the sample that falls below some size limit, and the percent of the sample that falls above some size limit.1.1 These test methods cover the determination of the physical and chemical properties of powdered ion exchange resins and are intended for use in testing new materials. The following test methods are included: SectionsTest Method A—Particle Size Distribution 5 to 15Test Method B—Solids Content 16 to 231.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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1.1 This document covers terminology relating to engine coolants. It is intended to provide a reference for anyone seeking information on engine coolants, and also to provide a uniform set of definitions for use in preparing ASTM specifications, test methods and other standard documents.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
5.1 Determination of the color of petroleum products is used mainly for manufacturing control purposes and is an important quality characteristic because color is readily observed by the user of the product. In some cases the color may serve as an indication of the degree of refinement of the material. When the color range of a particular product is known, a variation outside the established range may indicate possible contamination with another product. However, color is not always a reliable guide to product quality and should not be used indiscriminately in product specifications.1.1 This test method covers the automatic determination of color of a wide variety of petroleum products such as undyed motor and aviation gasoline, aviation turbine fuels, naphthas, kerosine, pharmaceutical white oils, diesel fuel oils, heating oils, and lubricating oils by the automatic tristimulus method. This test method correlates to Test Method D156 and Test Method D1500 as calculated by the instrumentation.NOTE 1: With the appropriate sample handling, this test method would apply to petroleum waxes, but they were not used in the round robin, and the precision of this test method with regard to waxes is unknown.1.2 This test method reports results in terms of Test Method D156 or Test Method D1500.1.3 This test method has a one-to-one correlation for the entire range of Test Method D1500 ASTM Color and for the range from 0 to +30 for Test Method D156 Saybolt color.1.4 This test method does not apply to solid samples, petroleum products containing dye, and petroleum products having extreme fluorescence.1.5 This test method does not apply to cloudy samples. Such samples shall be filtered so they are clear before measuring.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
5.1 The quantitative determination of olefins in spark-ignition engine fuels is required to comply with government regulations.5.2 Knowledge of the total olefin content provides a means to monitor the efficiency of catalytic cracking processes.5.3 This test method provides better precision for olefin content than Test Method D1319. It also provides data in a much shorter time, approximately 20 min following calibration, and maximizes automation to reduce operator labor.5.4 This test method is not applicable to M85 or E85 fuels, which contain 85 % methanol and ethanol, respectively.1.1 This test method provides for the quantitative determination of total olefins in the C4 to C10 range in spark-ignition engine fuels or related hydrocarbon streams, such as naphthas and cracked naphthas. Olefin concentrations in the range from 0.2 % by liquid-volume or mass to 5.0 % by liquid-volume or mass, or both, can be determined directly on the as-received sample whereas olefins in samples containing higher concentrations are determined after appropriate sample dilution prior to analysis.1.2 This test method is applicable to samples containing alcohols and ethers; however, samples containing greater than 15 % alcohol must be diluted. Samples containing greater than 5.0 % ether must also be diluted to the 5.0 % or less level, prior to analysis. When ethyl-tert-butylether is present, only olefins in the C4 to C9 range can be determined.1.3 This test method can not be used to determine individual olefin components.1.4 This test method can not be used to determine olefins having higher carbon numbers than C10.NOTE 1: Precision was determined only on samples containing MTBE and ethanol.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
5.1 The quantitative determination of hindered phenol antioxidants in a new turbine oil measures the amount of this material that has been added to the oil as protection against oxidation. Beside phenols, turbine oils can be formulated with other antioxidants such as amines which can extend the oil life. In used oil, the determination measures the amount of original (phenolic) antioxidant remaining after oxidation have reduced its initial concentration. This test method is not designed or intended to detect all of the antioxidant intermediates formed during the thermal and oxidative stressing of the oils, which are recognized as having some contribution to the remaining useful life of the used or in-service oil. Nor does it measure the overall stability of an oil, which is determined by the total contribution of all species present. Before making final judgment on the remaining useful life of the used oil, which might result in the replacement of the oil reservoir, it is advised to perform additional analytical techniques (in accordance with Practices D6224 and D4378), having the capability of measuring remaining oxidative life of the used oil.5.1.1 This test method is applicable to non-zinc turbine oils. These are refined mineral oils containing rust and oxidation inhibitors, but not antiwear additives. This test method has not yet been established with sufficient precision for antiwear oils.5.2 This test method is also suitable for manufacturing control and specification acceptance.5.3 When a voltammetric analysis is obtained for a turbine oil inhibited with a typical hindered phenol antioxidant, there is an increase in the current of the produced voltammogram between 3 s to 5 s (or 0.3 V to 0.6 V applied voltage) (see Note 1) in the basic test solution (Fig. 1—x-axis 1 second = 0.1 V). Hindered phenol antioxidants detected by voltammetric analysis include, but are not limited to, 2,6-di-tert-butyl-4-methylphenol; 2,6-di-tert-butylphenol and 4,4'-methylenebis(2,6-di-tert-butylphenol).NOTE 1: Voltages listed with respect to reference electrode. The voltammograms shown in Figs. 1 and 2 were obtained with a platinum reference electrode and a voltage scan rate of 0.1 V/s.FIG. 2 Amine and Hindered Phenols Peaks in the Basic Test Solution with Blank Response ZeroedNOTE 1: x-axis = time (seconds) and y-axis is current (arbitrary units). Top line in Fig. 2 is fresh oil, and lower line is used oil.5.4 For non-zinc turbine oils containing aromatic (aryl) amine compounds (antioxidants and corrosion inhibitors), there is an increase in the current of the produced voltammogram between 7 s to 11 s (0.7 V to 1.1 V applied voltage in Fig. 2) (see Note 1) which does not interfere with the hindered phenol measurement in the basic test solution. For the measurement of these aromatic amine antioxidants, refer to Test Method D6971, where the neutral test solution shall be used.1.1 This test method covers the voltammetric determination of hindered phenol antioxidants in new or in-service non-zinc turbine oils in concentrations from 0.0075 % by weight up to concentrations found in new oils by measuring the amount of current flow at a specified voltage in the produced voltammogram.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
5.1 Graffiti on buildings and structures is a significant problem in various regions across the country. A variety of coatings have been developed to be either resistant to the application of paints/marker or to aid in their removal. This standard practice describes a procedure for evaluating the effectiveness of anti-graffiti coatings applied to various concrete, masonry and natural stone substrates. It does not address graffiti removal on metal or any other non-mineral substrate.5.2 This practice only addresses graffiti removal on substrates in a laboratory environment, that have not been exposed to either natural or artificial weathering. Specification D6578 describes a method for graffiti removal after both natural and artificial weathering.1.1 This practice covers a basic method for evaluating the performance of anti-graffiti products on mineral building substrates by a series of increasingly abrasive cleaning methods. The anti-graffiti materials are applied to a series of concrete, masonry and natural stone specimens for evaluation. Graffiti resistance is based on how a defined set of markings are removed by a designated set of cleaning techniques.1.2 This practice also defines a procedure to evaluate graffiti removal after re-marking with subsequent re-cleaning. It does not address the re-treatment of substrates after a material is no longer graffiti resistant.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
1.1 This specification covers minimum requirements for cellulose fibers intended for use in fiber-reinforced concrete, and other cementitious products.1.2 This specification provides for measurement of properties, definition of types, typical properties, and prescribes testing procedures to establish conformance to these requirements.1.3 In the case of conflict between a more stringent requirement of a product specification and a requirement of this specification, the product specification shall prevail. In the case of a conflict between a requirement of the product specification or a requirement of this specification and a more stringent requirement of the purchase order, the purchase order shall prevail. The purchase order requirements shall not take precedence if they, in any way, violate the requirements of the product specification or this specification; for example, by the waiving of a test requirement or by making a test requirement less stringent.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
4.1 This test method is based on the cold oxidation of the glycerol by sodium metaperiodate in a strong acidic medium. Formaldehyde and formic acid are produced in this reaction and the latter is used to measure the glycerol content by titration with standard sodium hydroxide solution, to a pH 8.1 ± 0.1. The glycerol content is expressed as a percentage (m/m).4.2 Interferences—The glycerin sample should be free of organic compounds with more than two hydroxyl groups on adjacent carbon atoms (for example, sugars, glycols). These types of compounds may produce formic acid which interferes with the determination of the glycerol content.1.1 This test method provides the quantitative determination of glycerin by the titrimetric method. It is applicable to all glycerin or glycerin/water mixtures >75 %.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns associated with its use. It is the responsibility of the user of this standard to consult the established and appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautions are listed in Section 8.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
4.1 To determine the characteristics of the asphalt in an asphalt paving mixture, it is necessary to extract the asphalt from the aggregate by means of a suitable solvent and then to recover the asphalt from the solvent without significantly changing the asphalt’s properties. The asphalt recovered from the solvent by this practice can be tested using the same methods as for the original asphalt cement, and comparisons between the properties of the original and recovered asphalt can be made.4.2 Users are cautioned that the recovered binder properties from an asphalt mixture sample may not exactly represent the properties of the original asphalt binder due to factors outside of laboratory control such as aging, contamination, and molecular changes caused by exposure to heat and solvents. Consequently, recovered asphalt binder properties should not be used as a basis for acceptance.NOTE 1: The quality of the results produced by this is dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, and so forth. Users of this practice are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.1.1 This practice is intended to be used to recover asphalt from a solvent using the rotary evaporator to ensure that changes in the asphalt properties during the recovery process are minimized.1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
1.1 This specification describes an alcohol-carboxylic acid blend, referred to as the microemulsion blendstock.1.1.1 Warning—The microemulsion blendstock should be stored in facilities and equipment designed for oxygenated and low flashpoint liquids.1.2 The microemulsion blendstock is to be blended with fuel oils to produce a microemulsion test fuel oil that consists of inverse micelles.NOTE 1: While no fuel standard currently exists for a microemulsion test fuel oil, work to develop one is underway.NOTE 2: Typical fuel oils that could be used for blending with microemulsion blendstock are fuels that comply with Specifications D975 and D396 and may contain up to 5 % by volume biodiesel.NOTE 3: Testing with test fuels containing 10 % microemulsion blendstock using B5 as a base fuel did not show any detrimental changes to specified fuel properties relative to B0 base fuels, but can impair measurement of microemulsion blendstock concentration.1.2.1 The microemulsion test fuel oil (to be made from this blendstock) is to be used for testing and demonstration purposes only in specific equipment and vehicles that are suited for or have been equipped with safety precautions for use with low flashpoint fuels and oxygenated fuels such as ethanol. Minimum safety precautions may include flame arrestors and grounding straps.NOTE 4: The low flash point of this blendstock relative to conventional diesel fuel increases certain hazards during storage and distribution.1.3 Nothing in this specification shall preclude observance of federal, state, or local regulations, which may be more restrictive.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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