5.1 The measurement of the resistance to abrasion of textile and other materials is very complex. The resistance to abrasion is affected by many factors, such as the inherent mechanical properties of the fibers; the dimensions of the fibers; the structure of the yarns; the construction of the fabrics; and the type, kind, and amount of finishing material added to the fibers, yarns, or fabric.5.2 The resistance to abrasion is also greatly affected by the conditions of the tests, such as the nature of abradant, variable action of the abradant over the area of specimen abraded, the tension of the specimen, the pressure between the specimen and abradant, and the dimensional changes in the specimens.5.3 Abrasion tests are all subject to variation due to changes in the abradant during specific tests. The abradant must accordingly be discarded at frequent intervals or checked periodically against a standard. With disposable abradants, the abradant is used only once or discarded after limited use. With permanent abradants that use hardened metal or equivalent surfaces, it is assumed that the abradant will not change appreciably in a specific series of tests. Similar abradants used in different laboratories will not change at the same rate, due to differences in usage. Permanent abradants may also change due to pick up of finishing or other material from test fabrics and must accordingly be cleaned at frequent intervals. The measurement of the relative amount of abrasion may also be affected by the method of evaluation and may be influenced by the judgment of the operator.5.4 The resistance of textile materials to abrasion as measured on a testing machine in the laboratory is generally only one of several factors contributing to wear performance or durability as experienced in the actual use of the material. While “abrasion resistance” (often stated in terms of the number of cycles on a specified machine, using a specified technique to produce a specified degree or amount of abrasion) and “durability” (defined as the ability to withstand deterioration or wearing out in use, including the effects of abrasion) are frequently related, the relationship varies with different end uses, and different factors may be necessary in any calculation of predicted durability from specific abrasion data. Laboratory tests may be reliable as an indication of relative end-use performance in cases where the difference in abrasion resistance of various materials is large, but they should not be relied upon where differences in laboratory test findings are small. In general, they should not be relied upon for prediction of actual wear-life in specific end uses unless there are data showing the specific relationship between laboratory abrasion tests and actual wear in the intended end-use.5.5 These general observations apply to all types of fabrics, including woven, nonwoven, and knit apparel fabrics, household fabrics, industrial fabrics, and floor coverings. It is not surprising, therefore, to find that there are many different types of abrasion testing machines, abradants, testing conditions, testing procedures, methods of evaluation of abrasion resistance and interpretation of results.5.6 All the test methods and instruments so far developed for measuring abrasion resistance may show a high degree of variability in results obtained by different operators and in different laboratories; however, they represent the test methods now most widely in use.5.7 Because there is a definite need for measuring the relative resistance to abrasion, standardized test methods are needed and useful and may clarify the problem and lessen the confusion.5.8 Because of the conditions mentioned above, technicians frequently fail to get good agreement between results obtained on the same type of testing instrument both within and between laboratories, and the precision of these test methods is uncertain.5.9 Test Method D3886 is not recommended for acceptance testing of commercial shipment because of the poor between-laboratory precision.5.9.1 In cases of a dispute arising from differences in reported test results when using this test method for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens which are as homogeneous as possible and which are from a lot of material of the type in question. The test specimens should then be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using appropriate statistical analysis for unpaired data and an acceptable probability level chosen by the two parties before the testing begins. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results in the light of the known bias.1.1 This test method2 covers the determination of the resistance to abrasion of woven and knitted textile fabrics, both conditioned and wet, using the inflated diaphragm tester. This procedure is not applicable to floor coverings.NOTE 1: Other procedures for measuring the abrasion resistance of textile fabrics are given in Test Methods D3884, D3885, D1175 and AATCC Test Method 93.1.2 The values stated in SI units are to be regarded as standard; the values in English units are provided as information only and are not exact equivalents.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
5.1 The presence of cyanogen chloride in chlorinated sanitary and industrial effluents and therefore receiving waters is of concern because of its toxicity to aquatic life.5.2 This test method provides an analytical procedure for measuring cyanogen chloride in water.5.3 This test method is applicable for clean metal finishing and chlorinated sanitary and industrial effluents, and also can be used to establish process control of cyanide destruction by chlorination in waste water treatment facilities.1.1 This test method covers the determination of cyanogen chloride in water. Cyanogen chloride is normally present only at very low concentrations; it is a very labile and sparsely soluble gaseous compound. Water samples may contain cyanogen chloride after the chlorination of waste waters containing cyanide or thiocyanate compounds.1.2 Cyanogen chloride is unstable. A quick test using a spot plate or comparator as soon as the sample is collected may be the best test, reducing the loss of cyanogen chloride during the time lapse between sampling and analysis. (See Fig. 1 for a typical decay curve for cyanogen chloride in a solution.)FIG. 1 Cyanogen Chloride Stability1.3 This test method has been used successfully with reagent water. The analyst is responsible for determining whether the test method is applicable to the water matrix being tested. Reference is made to Test Method D of Test Methods D2036 which is based on similar chemical reactions and has been evaluated by collaborative testing in this matrix.1.4 The lower limit of detectability is 0.005 mg CN −/L.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 8.5 and 8.7 and Section 9.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
7.1 The particle size distribution of powdered ion exchange resins and, more importantly, the derived parameters of mean particle size and percent above and below specified size limits are useful for determining batch to batch variations and, in some cases, can be related to certain aspects of product performance.7.2 Although automatic multichannel particle size analyzers, of the type described in Section 9, yield information on the entire distribution of sizes present in a given sample, it has been found that, for this application, the numerical value of three derived parameters may adequately describe the particle size characteristics of the samples: the mean particle diameter (in micrometres), the percent of the sample that falls below some size limit, and the percent of the sample that falls above some size limit.1.1 These test methods cover the determination of the physical and chemical properties of powdered ion exchange resins and are intended for use in testing new materials. The following test methods are included: SectionsTest Method A—Particle Size Distribution 5 to 15Test Method B—Solids Content 16 to 231.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
1.1 This document covers terminology relating to engine coolants. It is intended to provide a reference for anyone seeking information on engine coolants, and also to provide a uniform set of definitions for use in preparing ASTM specifications, test methods and other standard documents.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
5.1 Determination of the color of petroleum products is used mainly for manufacturing control purposes and is an important quality characteristic because color is readily observed by the user of the product. In some cases the color may serve as an indication of the degree of refinement of the material. When the color range of a particular product is known, a variation outside the established range may indicate possible contamination with another product. However, color is not always a reliable guide to product quality and should not be used indiscriminately in product specifications.1.1 This test method covers the automatic determination of color of a wide variety of petroleum products such as undyed motor and aviation gasoline, aviation turbine fuels, naphthas, kerosine, pharmaceutical white oils, diesel fuel oils, heating oils, and lubricating oils by the automatic tristimulus method. This test method correlates to Test Method D156 and Test Method D1500 as calculated by the instrumentation.NOTE 1: With the appropriate sample handling, this test method would apply to petroleum waxes, but they were not used in the round robin, and the precision of this test method with regard to waxes is unknown.1.2 This test method reports results in terms of Test Method D156 or Test Method D1500.1.3 This test method has a one-to-one correlation for the entire range of Test Method D1500 ASTM Color and for the range from 0 to +30 for Test Method D156 Saybolt color.1.4 This test method does not apply to solid samples, petroleum products containing dye, and petroleum products having extreme fluorescence.1.5 This test method does not apply to cloudy samples. Such samples shall be filtered so they are clear before measuring.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
5.1 The quantitative determination of olefins in spark-ignition engine fuels is required to comply with government regulations.5.2 Knowledge of the total olefin content provides a means to monitor the efficiency of catalytic cracking processes.5.3 This test method provides better precision for olefin content than Test Method D1319. It also provides data in a much shorter time, approximately 20 min following calibration, and maximizes automation to reduce operator labor.5.4 This test method is not applicable to M85 or E85 fuels, which contain 85 % methanol and ethanol, respectively.1.1 This test method provides for the quantitative determination of total olefins in the C4 to C10 range in spark-ignition engine fuels or related hydrocarbon streams, such as naphthas and cracked naphthas. Olefin concentrations in the range from 0.2 % by liquid-volume or mass to 5.0 % by liquid-volume or mass, or both, can be determined directly on the as-received sample whereas olefins in samples containing higher concentrations are determined after appropriate sample dilution prior to analysis.1.2 This test method is applicable to samples containing alcohols and ethers; however, samples containing greater than 15 % alcohol must be diluted. Samples containing greater than 5.0 % ether must also be diluted to the 5.0 % or less level, prior to analysis. When ethyl-tert-butylether is present, only olefins in the C4 to C9 range can be determined.1.3 This test method can not be used to determine individual olefin components.1.4 This test method can not be used to determine olefins having higher carbon numbers than C10.NOTE 1: Precision was determined only on samples containing MTBE and ethanol.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
5.1 The quantitative determination of hindered phenol antioxidants in a new turbine oil measures the amount of this material that has been added to the oil as protection against oxidation. Beside phenols, turbine oils can be formulated with other antioxidants such as amines which can extend the oil life. In used oil, the determination measures the amount of original (phenolic) antioxidant remaining after oxidation have reduced its initial concentration. This test method is not designed or intended to detect all of the antioxidant intermediates formed during the thermal and oxidative stressing of the oils, which are recognized as having some contribution to the remaining useful life of the used or in-service oil. Nor does it measure the overall stability of an oil, which is determined by the total contribution of all species present. Before making final judgment on the remaining useful life of the used oil, which might result in the replacement of the oil reservoir, it is advised to perform additional analytical techniques (in accordance with Practices D6224 and D4378), having the capability of measuring remaining oxidative life of the used oil.5.1.1 This test method is applicable to non-zinc turbine oils. These are refined mineral oils containing rust and oxidation inhibitors, but not antiwear additives. This test method has not yet been established with sufficient precision for antiwear oils.5.2 This test method is also suitable for manufacturing control and specification acceptance.5.3 When a voltammetric analysis is obtained for a turbine oil inhibited with a typical hindered phenol antioxidant, there is an increase in the current of the produced voltammogram between 3 s to 5 s (or 0.3 V to 0.6 V applied voltage) (see Note 1) in the basic test solution (Fig. 1—x-axis 1 second = 0.1 V). Hindered phenol antioxidants detected by voltammetric analysis include, but are not limited to, 2,6-di-tert-butyl-4-methylphenol; 2,6-di-tert-butylphenol and 4,4'-methylenebis(2,6-di-tert-butylphenol).NOTE 1: Voltages listed with respect to reference electrode. The voltammograms shown in Figs. 1 and 2 were obtained with a platinum reference electrode and a voltage scan rate of 0.1 V/s.FIG. 2 Amine and Hindered Phenols Peaks in the Basic Test Solution with Blank Response ZeroedNOTE 1: x-axis = time (seconds) and y-axis is current (arbitrary units). Top line in Fig. 2 is fresh oil, and lower line is used oil.5.4 For non-zinc turbine oils containing aromatic (aryl) amine compounds (antioxidants and corrosion inhibitors), there is an increase in the current of the produced voltammogram between 7 s to 11 s (0.7 V to 1.1 V applied voltage in Fig. 2) (see Note 1) which does not interfere with the hindered phenol measurement in the basic test solution. For the measurement of these aromatic amine antioxidants, refer to Test Method D6971, where the neutral test solution shall be used.1.1 This test method covers the voltammetric determination of hindered phenol antioxidants in new or in-service non-zinc turbine oils in concentrations from 0.0075 % by weight up to concentrations found in new oils by measuring the amount of current flow at a specified voltage in the produced voltammogram.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
5.1 Graffiti on buildings and structures is a significant problem in various regions across the country. A variety of coatings have been developed to be either resistant to the application of paints/marker or to aid in their removal. This standard practice describes a procedure for evaluating the effectiveness of anti-graffiti coatings applied to various concrete, masonry and natural stone substrates. It does not address graffiti removal on metal or any other non-mineral substrate.5.2 This practice only addresses graffiti removal on substrates in a laboratory environment, that have not been exposed to either natural or artificial weathering. Specification D6578 describes a method for graffiti removal after both natural and artificial weathering.1.1 This practice covers a basic method for evaluating the performance of anti-graffiti products on mineral building substrates by a series of increasingly abrasive cleaning methods. The anti-graffiti materials are applied to a series of concrete, masonry and natural stone specimens for evaluation. Graffiti resistance is based on how a defined set of markings are removed by a designated set of cleaning techniques.1.2 This practice also defines a procedure to evaluate graffiti removal after re-marking with subsequent re-cleaning. It does not address the re-treatment of substrates after a material is no longer graffiti resistant.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
1.1 This specification covers minimum requirements for cellulose fibers intended for use in fiber-reinforced concrete, and other cementitious products.1.2 This specification provides for measurement of properties, definition of types, typical properties, and prescribes testing procedures to establish conformance to these requirements.1.3 In the case of conflict between a more stringent requirement of a product specification and a requirement of this specification, the product specification shall prevail. In the case of a conflict between a requirement of the product specification or a requirement of this specification and a more stringent requirement of the purchase order, the purchase order shall prevail. The purchase order requirements shall not take precedence if they, in any way, violate the requirements of the product specification or this specification; for example, by the waiving of a test requirement or by making a test requirement less stringent.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
4.1 This test method is based on the cold oxidation of the glycerol by sodium metaperiodate in a strong acidic medium. Formaldehyde and formic acid are produced in this reaction and the latter is used to measure the glycerol content by titration with standard sodium hydroxide solution, to a pH 8.1 ± 0.1. The glycerol content is expressed as a percentage (m/m).4.2 Interferences—The glycerin sample should be free of organic compounds with more than two hydroxyl groups on adjacent carbon atoms (for example, sugars, glycols). These types of compounds may produce formic acid which interferes with the determination of the glycerol content.1.1 This test method provides the quantitative determination of glycerin by the titrimetric method. It is applicable to all glycerin or glycerin/water mixtures >75 %.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns associated with its use. It is the responsibility of the user of this standard to consult the established and appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautions are listed in Section 8.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.